Bulk Electrolysis GC Cell

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  • €790.00

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This is a single compartment bulk electrolysis cell (known also as potentiostatic coulometry cell or controlled potential coulometry cell). In this innovative cell concept, the cell vessel made of Glassy Carbon contains studied liquid and acts as a working electrode at the same time. The electrical connection to this electrode is made by 0.75 mm thick Copper ring pressed to the Glassy Carbon chamber by the lid. The counter electrode (typically Platinum wire or Platinum gauze electrode) and reference electrode (typically Ag/AgCl for aqueous electrolytes or Ag/Ag+ for organic media) are installed in the cell lid. Both counter and reference electrodes are not included in the cell and should be added to the quotation separately. Glassy Carbon working electrode provides a large flat surface area which is easy to clean (chemically and mechanically). This unique electrode arrangement and possibility to use magnetic stirring ensure very efficient mass transport conditions and multiple use. The cell is insulated from the bottom by PTFE cup and can be placed on a metallic surface such as stirring plate or hot plate. The cell elements are constructed with materials that are inert to the sample (PEEK and PTFE). It well fits aqueous (EPDM O-Rings) and organic solvent (FFKM O-Rings) electrolyte requirements. The construction is liquid- and gas-tight. 

Application note
Usually electrolysis is carried out under potentiostatic conditions by stepping the potential from a value where no faradaic current is observed to one where the reaction is mass transport-controlled. Typical applications of bulk electrolysis include complete oxidation or reduction of species, the complete synthesis of a product through electrochemical processes (small-scale preparative electrosynthesis and electroseparation), partial oxidation or reduction of a compound to change the ratio of oxidized and reduced species and studying the complexity of the reaction mechanism (e.g. coupled reactions).

Specification
electrode plug diameter: 6 mm
lid entry depth: 8.25 mm
GC maximum temperature: 3000 °C (under vacuum or inert gas)
GC density: 1.42 g/cm3
GC open porosity: 0 %
GC permeability coefficient: 10-9 cm2/s
GC Vickers hardness: 230 HV
GC specific electrical resistance at 30 °C: 45 Ωµm
GC thermal conductivity at 30 °C: 6.3 W/(Km)
GC median linear coefficient of expansion (20-200 °C): 2.6x10
-6 1/K
Glassy Carbon chamber dimensions:

maximum liquid volume ID h (GC chamber depth) wall thickness number of ports
7 mL 19 mm 34 mm 3 mm 2 x 6 mm dia. port
15 mL 24 mm 42 mm 3 mm 2 x 6 mm dia. port
20 mL 30 mm 40 mm 3 mm 4 x 6 mm dia. port
40 mL 35 mm 51 mm 3 mm 4 x 6 mm dia. port
60 mL 34 mm 75 mm 5 mm 4 x 6 mm dia. port
90 mL 43 mm 73 mm 3 mm 4 x 6 mm dia. port
125 mL 50 mm 73 mm 3 mm 4 x 6 mm dia. port
250 mL 68 mm 79 mm 3 mm 4 x 6 mm dia. port
340 mL 61 mm 125 mm 3 mm 4 x 6 mm dia. port
790 mL 98 mm 113 mm 3 mm 4 x 6 mm dia. port

Product includes
1 x lid
1 x Glassy Carbon chamber
1 x working electrode contact (Copper)
1 or 3 x plug depending on variant
1 x insulating PTFE cup
1 x set of fittings
1 x set of O-Rings

Related products
Reference Electrodes
Metal Wire Auxiliary Electrodes
Non-metal Electrodes

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